Analysis of PFAS in Solid Waste

Two PFAS compounds, PFOA and PFOS have been named as hazardous substances under CERCLA allowing EPA to enforce monitoring and cleanup of contaminated sites. EPA has proposed including these and additional PFAS to RCRA regulations. The most used technique for PFAS analysis are Tandem Liquid Chromatography Mass Spectrometry or LC-MS/MS. Other approaches, such as single quadrupole LCMS, High Resolution LCMS, or GCMS may be used depending on the objectives of the analysis.

Adsorbable Organic Fluorine (AOF) is a screening method designed to detect additional PFAS compounds not captured by chromatographic methods. Fluorinated pesticides and pharmaceuticals may also be detected.

Shimadzu offers a variety of analytical solutions for PFAS testing in environmental samples in accordance with the following standardized methods.

EPA Method 1633, Revision A, Analysis of Per- and Polyfluoroalkyl Substances (PFAS) in Aqueous, Solid, Biosolids, and Tissue Samples by LC-MS/MS

ASTM D8421 Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances (PFAS) in Aqueous Matrices by Co-solvation followed by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS).

SW-846 Method 8327 Per-and Polyfluoroalkyl Substances by Liquid Chromatography/Tandem Mass Spectrometry

 

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LCMS-8065XE Triple Quadrupole LC-MS/MS for the Analysis of PFAS in Solid Waste

LCMS-8065XE Triple Quadrupole LC-MS/MS

This newly designed instrument features StreamFocus ESI and IonFocus™ to optimize ion transmission into the detector and minimize contamination by the matrix. This results in high sensitivity with enhanced instrument uptime and long-term stability of response. Concentrations as low as 1 ppt using cosolvation methods, such as ASTM D8421, are reliably measured.

LCMS-TQ RX Series Triple Quadrupole LC-MS/MS for the Analysis of PFAS in Solid Waste

LCMS-TQ RX Series Triple Quadrupole LC-MS/MS

Choose between three instruments to fit your sensitivity and budget needs with this highly reliable, and easy to operate instrument. The heat assisted electrospray ionization with corespray technology promotes highly efficient ionization of a wide range of target compounds. Use this instrument for EPA Method 1633A, ASTM D8421, and many other applications requiring LCMS analysis.

Quadrupole Time-of-Flight Liquid Chromatograph Mass Spectrometer for the analysis of PFAS in solid waste

Quadrupole Time-of -Flight Liquid Chromatograph Mass Spectrometer

The Shimadzu LCMS – 9050 is a high resolution LCMS instrument enabling non-targeted screening and identification of unknown pollutants in environmental samples.

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